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 Karl Franzens University Graz

Graz University of Technology 

2D and 3D SEM-based electron diffraction techniques as central tools for correlative microscopy to obtain new insights into microstructure physics and chemistry
Stefan Zaefferer
Max Planck Institute for Iron Research Duesseldorf
https://www.mpie.de/2890931/microscopy_and_diffraction
16:15 - 17:15 Tuesday 09 March 2021 TUG online

Video: https://tugraz.webex.com/meet/gerald.kothleitner

The scanning electron microscope (SEM) offers two electron diffraction techniques that allow to obtain comprehensive and quantitative information about the crystalline microstructure of materials, namely electron backscatter diffraction (EBSD) with all its facets and variations, and electron channelling contrast imaging (ECCI). EBSD is the basis of 2- and 3-dimensional orientation microscopy which allows characterization of microstructures in terms of crystal structure, crystal orientation, and elastic crystal distortions. ECCI, on the other hand enables direct observation of crystal lattice defects like dislocations, stacking faults, grain boundaries and elastic strain fields, in a way very similar to transmission electron microscopy but on bulk samples instead of thin foils.

Combining these highly quantitative techniques with other techniques, e.g. x-ray spectroscopy, cathodoluminescence, micro- and nano-mechanical testing, transmission electron microscopy, atom probe tomography, or chemical modifications builds up an amazingly powerful toolset to study numerous questions of materials science from the nano-scale all the way to the macro-scale.

In my presentation I will introduce two particularly comprehensive examples: in the first one 3D EBSD and ECCI are combined with APT, nano-SIMS, and TEM to understand the origin of grain boundary corrosion of stainless steels. The second example deals with the origin of hydrogen embrittlement in high-strength TWIP steels. Here ECCI, cross-correlation EBSD and in-situ micromechanical and chemical testing are combined to reveal the complex interaction of hydrogen with microstructures.